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::: 可授權專利

1,4–雙(二氟甲基)四氟苯之製備方法

創作型式:
發明
專利證號:
US7544846B1
發明人:
林俊旭、何潛淵、歐偉雄、王時俊(元欣科技)、周娟玉、涂潮州
國別:
美國
獲證日期:
2009/06/09
專利摘要:
A method for preparing a biphenylphosphonate compound of the following formula (I): wherein n is 2 or 3; Ar is a C 6-C16 aromatic group; which comprising (a) reacting an o-phenylphenol with a phosphorus trichloride in the presence of a zinc chloride catalyst to form a 6-chloro-6H-dibenz [c,e] [1,2]oxaphosphorin of the following formula (II); (b) reacting a polyhydroxybenzene compound of the formula (III) (HO) n—Ar  (III) wherein n and Ar are defined the same as the above, with the compound of formula (II) to form a compound of the following formula (IV) wherein n and Ar are defined the same as the above; and (c) oxidizing the compound of formula (IV) in the presence of water and ozone to form the compound of formula (I).
IPC國際分類號:
C07F000902